[유기공업화학실험] acid-base extraction with thin-layer chromatography

소개

"[유기공업화학실험] acid-base extraction with thin-layer chromatography"에 대한 내용입니다.

목차

1. Title
2. Date
3. Apparatus & Reagents
4. Procedure
5. Result
6. Discussion
7. Reference

본문내용

1. Title
추출과 TLC

2. Date

3. Apparatus & Reagents
1) Apparatus
-TLC plate
-TLC developing chamber
-pincette
-beaker
-stand and clamp
-separatory funnel
-30ml Erlenmeyer flask
-Capillary tube
-Spoid
-Measuring cylinder
-Plate
-UV lamp
-Filter paper
-Buchner funnel
-Balance
-Spatula
-Watch glass
-Suction flask
2) Reagents
<Table 1. 실험에 사용되는 시약>
NameFormulaM.W (g/mol)d (g/mL
Benzoic acid C6H5CO2H 122.12 1.32 122.4 249
4-methoxyphenol HOC6H4OCH3 124.17422 1.55 52.5 243
p-Chloroaniline ClC6H4NH2 127.57124 1.43 72.5 232
Naphthalene C10H8 128.174 0.975 80.3 217.97
Hydrochloric acid HCl 36.46 1.18 -27.32 110
Sodium hydroxide NaOH 39.997 2.13 318.4(328) 1390
Sodium bicarbonate NaHCO3 84.0066 2.20 50 851
Ethyl acetate (EA) CH3COOCH2CH3 88.11 0.9005 -83.67 77.15
Hexane C6H14 86.178 0.6606 -96 68.5
Ethyl ether (ether) (C4H5)2O 74.12 0.7135 -116.3 34.48

참고자료

· https://www.scienceall.com/%ec%b9%bc%eb%9f%bc%ed%81%ac%eb%a1%9c%eb%a7%88%ed%86%a0%ea%b7%b8%eb%9e%98%ed%94%bccolumn-chromatography/
· Column chromatography
· https://www.scienceall.com/%ec%a2%85%ec%9d%b4-%ed%81%ac%eb%a1%9c%eb%a7%88%ed%86%a0%ea%b7%b8%eb%9e%98%ed%94%bcpaper-chromatography/
· Paper chromatography
· https://www.scienceall.com/%ea%b0%80%ec%8a%a4%ed%81%ac%eb%a1%9c%eb%a7%88%ed%86%a0%ea%b7%b8%eb%9e%98%ed%94%bcgas-chromatography-2/
· Gas chromatography
· https://www.scienceall.com/%ea%b3%a0%ec%86%8d%ec%95%a1%ec%b2%b4%ed%81%ac%eb%a1%9c%eb%a7%88%ed%86%a0%ea%b7%b8%eb%9e%98%ed%94%bchigh-speed-liquid-chromatography-2/
· High speed liquid chromatography