[화공실험] FTIR-적외선 흡수 분광법에 의한 고분자의 분석 실험 발표

목차

1. 실험 FT-IR
01 Introduction
FT-IR이란?
02 Theory
FT-IR의 작동 원리
03 Advantages
FT-IR 사용의 이점
04 Sampling Technique
샘플 처리 방법
05 Results
실험 결과

2. Appendix
• 골드 나노 입자
• FT-IR 이외의 물질 분석 방법 (NMR, Mass Spectroscopy)

본문내용

FT-IR 이란?
• 간섭계를 이용하여 얻어지는 간섭줄무늬를 푸리에 변환하여 적외선 흡수 스펙트럼을 얻는 방법

FT-IR 분석 과정
간섭계 >> 시료 분석 >> 푸리에 변환

FT-IR 분석 과정 [푸리에 변환]
Interferogram
(Light Absorption for Each Mirror Position)
-Fourier Transformation→
Spectrum
(Light Absorption for Each Wavelength)

FT-IR의 이점
간편성, 신속성
불순물 검사
비파괴 검사

Sampling 기법
투과기법
반사기법

참고자료

· MEASURING THE COLOR OF A PAINT ON CANVAS DIRECTLY WITH EXTERNAL DIFFUSE REFLECTANCE USING THE AGILENT CARY 60 UV-VIS SPECTROPHOTOMETER/paolo teragni 등 3명/2013/Agilent Technologies
· Measuring the purity of low volumes of DNA at 4 °C using the Agilent Cary 60 UV-Vis spectrophotometer with fiber optics microprobe/Fyfe science,westlakes shore, Australia /2011/Agilent Technologies
· Simple, automated measurements of the photocatalytic properties of colorimetric species using the Agilent Cary 60 UV-Vis spectrophotometer with fiber optics/ Fyfe science,westlakes shore, Australia/2011/Agilent Technologies
· Photocatalytic Degradation of Methyl Blue Dye and Enhanced Antibacterial Properties of Treated Wool with ZrCL4 and Dyeing with Madder/ Department of textile Engineering-Islamic Azad University-South Tehran Branch, Iran./2015
· Microvolume Protein Concentration Determination using the NanoDrop 2000c Spectrophotometer
· Philippe Desjardins 등 3명/2009/Thermo scientific nanodrop product
· http://slideplayer.com/slide/5885988/
· https://blog.naver.com/0sungbum0/220840959266
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· https://chem.libretexts.org/Core/Physical_and_Theoretical_Chemistry/Spectroscopy/Vibrational_Spectroscopy/Infrared_Spectroscopy/How_an_FTIR_Spectrometer_Operates
· http://tcctech.co.kr/?module=file&act=procFileDownload&file_srl=2160&sid=ce2e9726f705a62a04a2f2ce1a177de9
· Spectroscopy: Organic Chemistry A Brief Course 13th edition; Hard, Hadad; Brooks/Cole
· http://chem.khu.ac.kr/contents/common/popup/download.html?bbs_cls_cd=006009&cid=11032110480993&file_nm=NMR_Lecture(Wade,_5th).ppt&home_id
·  https://www.thermofisher.com/kr/ko/home/industrial/spectroscopy-elemental-isotope-analysis/spectroscopy-elemental-isotope-analysis-learning-center/molecular-spectroscopy-information/ftir-information/ftir-sample-handling-techniques.html