수열합성법으로 제조된 나노막대 구조 WO3의 광촉매 효과 및 염료 흡착 반응

서지정보

· 발행기관 : 한국분말야금학회
· 수록지 정보 : 한국분말야금학회지 / 24권 / 6호
· 저자명 : 유수열, 남충희

목차

1. 서 론
2. 실험 방법
2.1. WO3 제조에 필요한 재료
2.2. 수열합성법을 이용한 WO3 나노막대 제조
2.3. SEM, TEM, XRD 등을 이용한 WO3 특성 평가
2.4. 제조된 WO3를 이용한 메틸렌블루 흡착 실험
2.5. 광촉매 실험
3. 결과 및 고찰
4. 결 론
References

영어초록

Transition-metal oxide semiconductors have various band gaps. Therefore, many studies have been conducted in various application fields. Among these, methods for the adsorption of organic dyes and utilization of photocatalytic properties have been developed using various metal oxides. In this study, the adsorption and photocatalytic effects of WO3 nanomaterials prepared by hydrothermal synthesis are investigated, with citric acid added in the hydrothermal process as a structure-directing agent. The nanostructures of WO3 are studied using transmission electron microscopy and scanning electron microscopy images. The crystal structure is investigated using X-ray diffraction patterns, and the changes in the dye concentrations adsorbed on WO3 nanorods are measured with a UV-visible absorption spectrophotometer based on Beer-Lambert’s law. The methylene blue (MB) dye solution is subjected to acid or base conditions to monitor the change in the maximum adsorption amount in relation to the pH. The maximum adsorption capacity is observed at pH 3. In addition to the dye adsorption, UV irradiation is carried out to investigate the decomposition of the MB dye as a result of photocatalytic effects. Significant photocatalytic properties are observed and compared with the adsorption effects for dye removal.

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