By reacting (E,E)-2,4-hexadien-1-ol with maleic anhydride, synthesize 1,3,3a,4,5,7a-hexahydro-5-methyl ... Other (MSDS) (E,E)-2,4-hexadien-1-ol, C6H10O [CAS No. 17102-64-6] 98.14 0.87 30.50 80.00 Soluble in toluene ... -1-ol in this exp.), and if it disappears completely, you can terminate the rxn.
Density sorbic alcohol (E,E-2,4-hexadien-1-ol) 98.14 0.40 g 4.1mmol 1 28-33 °C 80 °C 0.871 g/mL maleic ... 오늘 실험의 목표는 단일 단계에서 cyclohexene 유도체를 제공하는, 소르브산 알코올(E,E-2,4-hexadien-1-ol)(≒ 1,3-diene)과 말레산 무수물(maleic ... 무게를 측정한 25Ml R.B.F에 0.40 g의 (E,E)-2,4-hexadien-1-ol를 바로 무게를 재서 넣는다. 1.0 cm magnetic stir bar, 5ml의 toluene과
ABSTRACT: 본 실험에서는 trans, trans-2,4-hexadien-1-ol (1)과 maleic anhydride (2)을 이용하여 Diels-Alder 반응을 진행, ... (3aR,4S,5S,7aR)-5-methyl-3-oxo-1,3,3a,4,5,7a-hexahydroisobenzofuran-4-carboxylic acid (3)의 합성을 진행하였다. ... Diels-Alder 반응은 두 반응물의 파이 결합 2개가 diene과 dienophile을 연결하는 2개의 시그마 결합으로 바뀌어 육각 고리를 형성하는 반응으로, 1928년 1,4
Objectives: Diels-Alder reaction of (E,E)-2,4-hexadien-1-ol and maleic anhydride can be carried out to ... synthesize (3aR,4S,5S,7aR)-5-methyl-3-oxo-1,3,3a,4,5,7a-hexahydroisobenzofuran-4-carboxylic acid.Principles ... & Methods(1) Principles: Diels-Alder Reaction is a cycloaddition between a 1,3-diene and an electron-poor
of maleic anhydride and (E,E)-2,4-hexadien-1-ol. ... ,5S,7aR)-5-methyl-3-oxo-1,3,a,4,5,7ahexahydroisobenzofuran-4-carboxylic acid with the Diels-Alder reaction ... should discuss your interpretation of the experimental results.Experiments allowed the synthesis of (3aR,4S