Synthesis of 3-hexylthiopheneIntroduction- PurposeTo synthesize 3-hexylthiophene using Grignard ... performed in tetrahydrofuran or de-ethyl ether as a solvent.3. NiCl₂(dppp)It is 1,3-Bis ... , weighing paper, analytical balance2. Reagent3-Bromothiophene, Hexylmagnesium bromide, Ni catalyst
Synthesis of Poly(3-hexylthiophene)Introduction- Purpose of the ExperimentTo obtain poly(3 ... Experimental Set-up1. PolymerizationDissolve 2,5-dibromo-3-hexylthiophene in the schlenk flask in THF in the ... poly(3-hexylthiophene) via NMR.Result & DiscussionIn the experiment, poly(3-hexylthiophene) was s
- Purpose of the ExperimentTo obtain 3-hexylthiophene through work-up and purification from ... reaction mixture synthesized using 3-bromothiophene, hexylmagnesium bromide, Ni catalyst, and THF. ... - Theoretical Background1.Work-upWork-up means the manipulation necessary to separate and purify the product